Key Engineering Materials, Volume 856 KEM, Pages 182-189 , 01/01/2020

Catalytic oxidation of furfural to succinic acid in the presence of sulfonic resins

Wipawan Kingkaew, Thanis Kaewwiset, Uthen Thubsuang, Chairat Siripattana, Kamchai Nuithitikul

Abstract

This research investigates the application of three sulfonic resins (Amberlyst-15, Dowex-G26 and Dowex Monosphere-650C) having different porous characteristics as acid heterogeneous catalysts for oxidation reaction of furfural with hydrogen peroxide solution. The reaction was carried out in a batch reactor with varied reaction time (4-24 h) and temperature (70-90<sup>o</sup> C). The sulfonic resins were characterized as to their structure and chemical composition by N2 adsorption isotherm, Fourier transformed-infrared (FTIR) spectroscopy, acid-base titration, and scanning electron microscopy (SEM). The results showed that all three resins gave similar catalytic activities. The highest yield of succinic acid was 75.7 % in the presence of Dowex-G26 catalyst at 80<sup>o</sup> C and 4 h.

Document Type

Conference Paper

Source Type

Book Series

ISBN

[9783035716726]

ISSN

10139826, 16629795

Keywords

AmberlystDowexFurfuralOxidationSuccinic acid

ASJC Subject Area

Materials Science : Materials Science (all)Engineering : Mechanics of MaterialsEngineering : Mechanical Engineering

Funding Agency

National Research Council of Thailand


Bibliography


Kingkaew, W., Kaewwiset, T., Thubsuang, U., Siripattana, C., & Nuithitikul, K. (2020). Catalytic oxidation of furfural to succinic acid in the presence of sulfonic resins. Key Engineering Materials, 856 KEM182-189. doi:10.4028/www.scientific.net/KEM.856.182

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