Ceramics International, Volume 37, Issue 1, Pages 333-340 , 01/01/2011

Synthesis, characterization and optical properties of Zn 1-xTixO nanoparticles prepared via a high-energy ball milling technique

Sumetha Suwanboon, Pongsaton Amornpitoksuk, Phuwadol Bangrak

Abstract

Zn<inf>1-x</inf>Ti<inf>x</inf>O (x = 0, 0.01, 0.03 and 0.05) nanoparticles were prepared by high-energy ball milling at 400 rpm. The milled powders were characterized by X-ray diffractometer (XRD) and the results exhibited that Ti-doped ZnO nanoparticles consisted of single phase with hexagonal structure when the mixtures of ZnO and TiO<inf>2</inf> powders were milled for 20 h. The crystallite size reduced as a function of the doping content and milling time from 1 to 10 h then increased after milling for 20 h and when the annealing temperature increased. The strain changed inversely to the crystallite size. A wider band-gap was obtained by increasing the doping content and annealing temperature because of a reduction in defect concentration. Both ZnO- and Ti-doped ZnO nanoparticles caused damage to S. aureus, E. coli, P. mirabilis, S. typhi and P. aeruginosa. © 2010 Elsevier Ltd and Techna Group S.r.l.

Document Type

Article

Source Type

Journal

Keywords

A. MillingA. PowderB. X-ray diffractionD. ZnO

ASJC Subject Area

Materials Science : Electronic, Optical and Magnetic MaterialsMaterials Science : Surfaces, Coatings and FilmsChemical Engineering : Process Chemistry and TechnologyMaterials Science : Materials ChemistryMaterials Science : Ceramics and Composites


Bibliography


Suwanboon, S., Amornpitoksuk, P., & Bangrak, P. (2011). Synthesis, characterization and optical properties of Zn 1-xTixO nanoparticles prepared via a high-energy ball milling technique. Ceramics International, 37(1) 333-340. doi:10.1016/j.ceramint.2010.08.039

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